FlowSyn Continuous Flow Reactor

FlowSyn continuous flow reactor is designed for preparative scale flow chemistry. Two high pressure pumps are used to introduce reagents from bottles (or injection loops) to the reactors. Reactions can be heated to 260 °C and 150 °C in a coil and microreactor respectively. Back pressure regulators of up to 1000 psi can be used to superheat solvents, allowing the chemist to perform ’microwave like’ conditions with no limit on scale.

  

                  FlowSyn Microreactor


o Chemical inert
o Easy-to-use
o Rapid mixing

FlowSyn is very easy to use with a high resolution user interface. The user is guided through setting up a flow chemistry reaction by inputting parameters for reagent volumes, temperatures and reaction times. The user can choose to collect all of the reaction plug, or only the ’steady state’ part. FlowSyn will then equilibrate and run the reaction and finish with a solvent wash. FlowSyn will monitor the pressure of the system, and shut down safely if a problem occurs allowing FlowSyn to be run unattended.

 

FutureChemistry FlowScreen  




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Benefits		  
Features
  •  
    		• Efficiency - Offers complete unattended operation. System will equilibrate, run reaction and clean automatically
  •  
    		• Easy to use - Flow reaction parameters can be quickly entered via the intuitive user interface

  •  
    		• Safety - All pressurised parts are located behind a safety shield. Active pressure monitoring system as standard

  •  
    		• Versatile - The FlowSyn can be quickly reconfigured to perform a range of different flow chemistries

  •  
    		• Space saving - Compact footprint, fully integrated standard system
    		 
  • Max. 260 °C and 1000 psi

  • Exchangable reactors

  • Integrated user interface

  • ’Microwave like’ conditions

  • mg to 100’s g’s scale

  • Increase capability with extra modules


    • Applications
    Selection of chemical reactions which have been carried out succesfully in the FlowSyn:

  • Bromination
  • Bohlmann-Rahtz Pyridine Synthesis
  • ’Catch and Release’ Array Synthesis
  • Condensation Reaction
  • Ester Hydrolysis under Segmented Plug Flow Conditions
  • Curtius Rearrangement
  • Scale-up Synthesis of a Zyvox Intermediate
  • Chlorothiobenzimidazolinone Synthesis
  • 2-Thiobenzimidazolinone Synthesis
  • Esterification
  • Knorr Pyrazole Synthesis
  • Ester Hydrolysis
  • SNAR Reaction


    Visit our webshop or call +31  (0) 24 711 4029 for a free quotation.

     

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